Technology Process of 2-(2-benzoyloxy-5-hydroxypentyl)-1-(t-butoxycarbonyl)pyrrolidine
There total 5 articles about 2-(2-benzoyloxy-5-hydroxypentyl)-1-(t-butoxycarbonyl)pyrrolidine which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
formic acid;
palladium on activated charcoal;
In
methanol;
for 2h;
Ambient temperature;
DOI:10.1246/bcsj.69.2063
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 92 percent / Et3N, NaI / acetonitrile / 8 h / 50 °C
2: 86 percent / CAN, MS 4a / various solvent(s) / 2 h
3: 100 percent / H2 / 10percent Pd/C / methanol / 5 h / 760 Torr / Ambient temperature
4: 90 percent / NaBH4 / tetrahydrofuran; methanol / 2 h / Ambient temperature
5: 100 percent / Py / 5 h / Ambient temperature
6: 100 percent / HCO2H / 10percent Pd/C / methanol / 2 h / Ambient temperature
With
pyridine; sodium tetrahydroborate; formic acid; ammonium cerium(IV) nitrate; hydrogen; triethylamine; sodium iodide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; acetonitrile;
DOI:10.1246/bcsj.69.2063
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / Py / 5 h / Ambient temperature
2: 100 percent / HCO2H / 10percent Pd/C / methanol / 2 h / Ambient temperature
With
pyridine; formic acid;
palladium on activated charcoal;
In
methanol;
DOI:10.1246/bcsj.69.2063
