6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine

Base Information

Chemical Name:6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine
CAS No.:64906-09-8
Molecular Formula:C₁₈H₂₁NO₂
Molecular Weight:283.37
Hs Code.:

6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenz<c,e>azocine

Synonyms:6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine

Chemical Property:

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Technology Process of 6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine

There total 2 articles about 6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.4%

: 116760-17-9
(2-Bromo-benzyl)-[2-(2-bromo-4,5-dimethoxy-phenyl)-ethyl]-methyl-amine

: 64906-09-8
6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine

: 96025-46-6
N-methyl-N-benzyl-3,4-dimethoxyphenethylamine

: Benzyl-[2-(2-bromo-4,5-dimethoxy-phenyl)-ethyl]-methyl-amine

Guidance literature:: With potassium iodide; bis(triphenylphosphine)nickel(II) chloride; triphenylphosphine; zinc; In N,N-dimethyl-formamide; at 55 ℃;

Reference yield:

: 63375-81-5
2-(2-bromo-4,5-dimethoxyphenylphenyl)ethan-1-amine

: 64906-09-8
6-methyl-10,11-dimethoxy-5,6,7,8-tetrahydrodibenzazocine

Guidance literature:: Multi-step reaction with 3 steps

1: 2.) NaBH₄ / 1.) 120 deg C, 2.5 h, 2.) CHCl₃, EtOH, r.t., 8 h

2: 1.) H₃BO₃, 2.) NaBH₄ / 1.) CH₃OH, H₂O, r.t.

3: 46.9 percent / KI / Ni(PPh₃)2Cl₂-Zn-PPh₃ / dimethylformamide / 55 °C

With sodium tetrahydroborate; boric acid; potassium iodide; bis(triphenylphosphine)nickel(II) chloride; triphenylphosphine; zinc; In N,N-dimethyl-formamide;