Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester

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Chemical Name:Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester
CAS No.:849482-36-6
Molecular Formula:C₂₃H₂₃NO₅
Molecular Weight:393.439
Hs Code.:

Synonyms:Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester

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Chemical Property of Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester

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Technology Process of Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester

There total 2 articles about Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 113489-84-2
(2'R,3'S,4R,5S)-3-(3'-hydroxy-2'-methyl-1'-oxo-5'-pentenyl)-4-methyl-5-phenyl-2-oxazolidone

: 65-85-0,8013-63-6
benzoic acid

: 849482-36-6
Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In benzene; at 20 ℃; for 12h;
DOI:10.1021/ol0500160

Reference yield:

: 77877-20-4
(4R,5S)-4-methyl-5-phenyl-3-propionyloxazolidin-2-one

: 849482-36-6
Benzoic acid (R)-1-[(R)-1-methyl-2-((4R,5S)-4-methyl-2-oxo-5-phenyl-oxazolidin-3-yl)-2-oxo-ethyl]-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-Bu₂BOTf; DIPEA / CH₂Cl₂ / 0.25 h / 0 °C

1.2: 77 percent / CH₂Cl₂ / 2 h / -78 - 0 °C

2.1: 96 percent / DEAD; PPh₃ / benzene / 12 h / 20 °C

With di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; diethylazodicarboxylate; In dichloromethane; benzene; 2.1: Mitsunobu reaction;
DOI:10.1021/ol0500160