(E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Base Information

Chemical Name:(E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid
CAS No.:212262-55-0
Molecular Formula:C₁₉H₁₉NO₈
Molecular Weight:389.362
Hs Code.:

Synonyms:(E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Suppliers and Price of (E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

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Technology Process of (E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

There total 2 articles about (E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 31680-08-7
4-methoxy-3-nitrobenzaldehyde

: 212262-55-0
(E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Guidance literature:: 3,4,5-trimethoxyphenyl acetic acid; 4-methoxy-3-nitrobenzaldehyde; With acetic anhydride; triethylamine; at 140 ℃; for 12h;

With hydrogenchloride; In water;
DOI:10.1016/j.bmc.2011.06.017

Reference yield: 44.0%

: 951-82-6
3,4,5-trimethoxyphenyl acetic acid

: 31680-08-7
4-methoxy-3-nitrobenzaldehyde

: (Z)-3-(4'-methoxy-3'-nitrophenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

: 212262-55-0
(E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

Guidance literature:: With acetic anhydride; triethylamine; at 140 ℃; for 20h;
DOI:10.1016/j.bmc.2005.02.039

Reference yield: 97.0%

: 155252-35-0
4β-amino-4-deoxypodophyllotoxin

: 212262-55-0
(E)-3-(3'-nitro-4'-dimethoxyphenyl)-2-(3'',4'',5''-trimethoxyphenyl)acrylic acid

: 1322005-57-1
4β-((E)-3-(4-methoxy-3-nitrophenyl)-2-(3,4,5-trimethoxyphenyl)acrylamido)-4-deoxypodophyllotoxin

Guidance literature:: With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 27 ℃; for 3h;