3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene

Base Information

Chemical Name:3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene
CAS No.:856668-86-5
Molecular Formula:C₂₂H₃₇BO₂S₂
Molecular Weight:408.478
Hs Code.:

Synonyms:3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene

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Chemical Property of 3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene

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Technology Process of 3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene

There total 1 articles about 3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 76-09-5
2,3-dimethyl-2,3-butane diol

: 121-43-7,63156-11-6
Trimethyl borate

: 856668-85-4
3,5-bis(tert-butylsulfidomethyl)bromobenzene

: 856668-86-5
3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene

Guidance literature:: With CH₃COOH; t-butyllithium; In diethyl ether; hexane; (N2); using Schlenk techniques; addn. of t-BuLi (2 equiv.)/hexane to BrC6H3(CH2SCMe3)2/Et2O at -78°C; stirring for 20 min, addn. of B(OMe)3 (1.5 equiv.); warming to room temp. overnight; addn. of pinacol for 10 min and then HOAc; stirring for 1 h; evapn. of solvent in vac., washing with MeOH, evapn. to dryness, elem. anal.;
DOI:10.1021/om050144s

Reference yield: 78.0%

: 856668-86-5
3,5-bis(tert-butylsulfidomethyl)pinacolboranebenzene

: 856668-66-1,856925-20-7
cis-[Pt(C₆H₃Br-4-((dimethylamino)methyl)-2)2]

: 856668-87-6
cis-[Pt(C₆H₃(C₆H₃(CH₂S(tert-butyl))2)-4-((dimethylamino)methyl)-2)]

Guidance literature:: With sodium carbonate; [1,1'-bis(diphenylphosphino)ferrocene]dichloropalladium(II); In tetrahydrofuran; 1,2-dimethoxyethane; water; (N2); introduction of Pt(NMe2CH2C6H3Br)2, ((CH3)2CO)2BC6H3(CH2SCMe3)2, PdCl2(dppf) and Na2CO3 into Schlenk flask; evacuating for 30 min, addn. of DME, THF and H2O; stirring at 70°C for 3 h; cooling to room temp., extn. with CH2Cl2, dryig over MgSO4, evapn. to dryness, chromy. (basic alumina, CH2Cl2); washing with hexane and Et2O, elem. anal.;
DOI:10.1021/om050144s