E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

Base Information

Chemical Name:E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol
CAS No.:290820-43-8
Molecular Formula:C₁₆H₂₆O₂SSi
Molecular Weight:310.533
Hs Code.:

Synonyms:E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

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Chemical Property of E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

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Technology Process of E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

There total 5 articles about E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 290820-49-4
E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiolacetate

: 290820-43-8
E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

Guidance literature:: With lithium aluminium tetrahydride; cesium chloride; In diethyl ether; at 20 ℃;
DOI:10.1016/S0968-0896(00)00037-7

Reference yield:

: 458-36-6
trans-coniferyl aldehyde

: 290820-43-8
E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / pyridine / 20 °C

2: 81 percent / CeCl₃; NaBH₄ / tetrahydrofuran

3: 95 percent / Ph₃P; diisopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

4: 93 percent / LiAlH₄; cesium chlorire / diethyl ether / 20 °C

With pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; di-isopropyl azodicarboxylate; cesium chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; 1: silylation / 2: Reduction / 3: Substitution / 4: Reduction;
DOI:10.1016/S0968-0896(00)00037-7

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 290820-43-8
E-4-O-(tert-butyldimethylsilyl)-3-methoxycinnamyl thiol

Guidance literature:: Multi-step reaction with 4 steps

1: 72 percent / pyridine / 20 °C

2: 81 percent / CeCl₃; NaBH₄ / tetrahydrofuran

3: 95 percent / Ph₃P; diisopropyl azodicarboxylate / tetrahydrofuran / 0 - 20 °C

4: 93 percent / LiAlH₄; cesium chlorire / diethyl ether / 20 °C

With pyridine; sodium tetrahydroborate; lithium aluminium tetrahydride; cerium(III) chloride; di-isopropyl azodicarboxylate; cesium chloride; triphenylphosphine; In tetrahydrofuran; diethyl ether; 1: silylation / 2: Reduction / 3: Substitution / 4: Reduction;
DOI:10.1016/S0968-0896(00)00037-7