(S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

Base Information

Chemical Name:(S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester
CAS No.:157435-81-9
Molecular Formula:C₁₇H₂₅NO₅
Molecular Weight:323.389
Hs Code.:

Synonyms:(S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

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Technology Process of (S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

There total 3 articles about (S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15026-17-2
succinic acid mono-tert-butyl ester

: 157435-81-9
(S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

Guidance literature:: Multi-step reaction with 3 steps

2: 90 percent / H₂ / S-Ru-BINAP / methanol; tetrahydrofuran / 20 h / 65 °C / 2585.7 Torr

3: 1.) Me₃Al / 1.) CH₂Cl₂, hexane, ice bath cooling to r.t., 1 h, 2.) CH₂Cl₂, overnight

With hydrogen; trimethylaluminum; S-Ru-BINAP; In tetrahydrofuran; methanol;
DOI:10.1021/jo00096a031

Reference yield:

: 93740-92-2
Hexanedioic acid 3-oxo-1-methyl-6-(1,1-dimethylethyl)ester

: 157435-81-9
(S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂ / S-Ru-BINAP / methanol; tetrahydrofuran / 20 h / 65 °C / 2585.7 Torr

2: 1.) Me₃Al / 1.) CH₂Cl₂, hexane, ice bath cooling to r.t., 1 h, 2.) CH₂Cl₂, overnight

With hydrogen; trimethylaluminum; S-Ru-BINAP; In tetrahydrofuran; methanol;
DOI:10.1021/jo00096a031

Reference yield:

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 157435-79-5
(S)-Hexanedioic acid 3-hydroxy-1-methyl-6-(1,1-dimethylethyl)ester

: 157435-81-9
(S)-Hexanoic acid 4-hydroxy-6-oxo-6-<(phenylmethoxy)amino>-(1,1-dimethylethyl) ester

Guidance literature:: With trimethylaluminum; Yield given. Multistep reaction; 1.) CH₂Cl₂, hexane, ice bath cooling to r.t., 1 h, 2.) CH₂Cl₂, overnight;
DOI:10.1021/jo00096a031