Technology Process of C21H20N2O3
There total 4 articles about C21H20N2O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
water; lithium hydroxide;
In
tetrahydrofuran;
at 20 ℃;
for 3h;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: caesium carbonate / N,N-dimethyl-formamide / 40 °C / Inert atmosphere
2: water; lithium hydroxide monohydrate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; water; caesium carbonate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.3390/molecules19010102
- Guidance literature:
-
Multi-step reaction with 3 steps
1: zinc acetate hydrate / methanol / 16 h / 20 °C / Inert atmosphere
2: caesium carbonate / N,N-dimethyl-formamide / 40 °C / Inert atmosphere
3: water; lithium hydroxide monohydrate / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere
With
lithium hydroxide monohydrate; zinc acetate hydrate; water; caesium carbonate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.3390/molecules19010102