N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester

Base Information

• Chemical Name: N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester
• CAS No.: 353757-53-6
• Molecular Formula: C₂₀H₂₀ClIN₂O₄
• Molecular Weight: 514.747

Synonyms:N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester

Chemical Property of N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester

Chemical Property:

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Technology Process of N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester

There total 2 articles about N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid chloromethyl ester (353757-50-3) → N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester (353757-53-6)

Guidance literature:

With sodium iodide; In acetone; at 30 ℃; for 3h;

DOI:10.1055/s-2002-19296

Reference yield:

halofenozide (112226-61-6) → N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester (353757-53-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: t-BuOK / tetrahydrofuran / 1 h

1.2: 85 percent / tetrahydrofuran / 1 h / 20 °C

2.1: 93 percent / NaI / acetone / 3 h / 30 °C

With potassium tert-butylate; sodium iodide; In tetrahydrofuran; acetone;

DOI:10.1055/s-2002-19296

Reference yield: 91.0%

acetic acid (64-19-7,77671-22-8) + N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid iodomethyl ester (353757-53-6) → acetic acid N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazinocarbonyloxy-methyl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1055/s-2002-19296

upstream raw materials:

N'-benzoyl-N'-tert-butyl-N-(4-chlorobenzoyl)hydrazine-carboxylic acid chloromethyl ester

halofenozide

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