N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

Base Information

Chemical Name:N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)
CAS No.:4932-23-4
Molecular Formula:C₂₈H₂₈N₂O₄S₄
Molecular Weight:584.805
Hs Code.:

Synonyms:N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

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Technology Process of N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

There total 2 articles about N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 52411-33-3,85340-40-5
1,4-bis(2-aminophenyl)-1,4-dithiabutane

: 98-59-9
p-toluenesulfonyl chloride

: 4932-23-4
N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

Guidance literature:: With pyridine; at -5 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.jorganchem.2010.01.030

Reference yield:

: 4932-23-4
N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

Guidance literature:: 2,2'-Etylendithioanilin, entspr. Sulfonsaeurechlorid;

Reference yield: 54.0%

: 4932-23-4
N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

: 1,2-bis(2-iodomercaptoethyl)-4,5-dicyanobenzene

: 1228078-05-4
13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

Guidance literature:: N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide); With potassium carbonate; In acetonitrile; at 50 - 85 ℃; Inert atmosphere;

1,2-bis(2-iodomercaptoethyl)-4,5-dicyanobenzene; In acetonitrile; for 120h; Inert atmosphere; Reflux;
DOI:10.1016/j.jorganchem.2010.01.030