13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

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Chemical Name:13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile
CAS No.:1228078-05-4
Molecular Formula:C₄₀H₃₆N₄O₄S₆
Molecular Weight:829.146
Hs Code.:

13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

Synonyms:13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

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Chemical Property of 13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

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Technology Process of 13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

There total 1 articles about 13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 4932-23-4
N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide)

: 1,2-bis(2-iodomercaptoethyl)-4,5-dicyanobenzene

: 1228078-05-4
13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

Guidance literature:: N,N-[ethane-1,2-diylbis(thio-2,1-phenylene)]bis(4-methylbenzene sulfonamide); With potassium carbonate; In acetonitrile; at 50 - 85 ℃; Inert atmosphere;

1,2-bis(2-iodomercaptoethyl)-4,5-dicyanobenzene; In acetonitrile; for 120h; Inert atmosphere; Reflux;
DOI:10.1016/j.jorganchem.2010.01.030

Reference yield: 37.0%

: 1228078-05-4
13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

: C₁₆₀H₁₄₄CoN₁₆O₁₆S₂₄

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; cobalt(II) chloride; at 175 ℃; for 0.15h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.jorganchem.2010.01.030

Reference yield: 36.0%

: 1228078-05-4
13,24-bis[(4-methylphenyl)sulfonyl]-6,7,14,15,23,24-hexahydro-13H,22H-tribenzo[b,h,n][1,4,10,13,7,16]tetrathiadiazacyclooctadecine-18,19,dicarbonitrile

: C₁₆₀H₁₄₄N₁₆NiO₁₆S₂₄

Guidance literature:: With 2-(N,N-dimethylamino)ethanol; nickel dichloride; at 175 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;
DOI:10.1016/j.jorganchem.2010.01.030