Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester

Base Information

Chemical Name:Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester
CAS No.:81380-11-2
Molecular Formula:C₁₉H₂₄O₅S
Molecular Weight:364.463
Hs Code.:

Synonyms:Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester

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Chemical Property of Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester

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Technology Process of Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester

There total 3 articles about Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 81380-11-2
Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH; 2.) 80percent aq. HOAc / 1.) THF, r.t.; 2.) r.t., 6 h

2: 1.) p-anisidyldiphenylmethylchoride; 3.) 80percent aq. HOAC

With sodium hydride; acetic acid; mono-4-methoxytrityl chloride;
DOI:10.1139/v82-016

Reference yield:

: 57280-24-7,57395-53-6,58967-01-4,69743-60-8,71565-21-4,74243-88-2,74243-89-3,85026-76-2
(R)-2-((S)-2,2-Dimethyl-[1,3]dioxolan-4-yl)-propan-1-ol

: 81380-11-2
Toluene-4-sulfonic acid (1S,2R)-3-benzyloxy-1-hydroxymethyl-2-methyl-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH; 2.) 80percent aq. HOAc / 1.) THF, r.t.; 2.) r.t., 6 h

2: 1.) p-anisidyldiphenylmethylchoride; 3.) 80percent aq. HOAC

With sodium hydride; acetic acid; mono-4-methoxytrityl chloride;
DOI:10.1139/v82-016