5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

Base Information

Chemical Name:5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide
CAS No.:121612-80-4
Molecular Formula:C₁₉H₂₁N₂O₂S*I
Molecular Weight:468.358
Hs Code.:

Synonyms:5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

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Chemical Property of 5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

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Technology Process of 5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

There total 8 articles about 5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 117390-38-2
thieno<2,3-b>pyridine-5-carboxylic acid

: 121612-80-4
5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

Guidance literature:: Multi-step reaction with 3 steps

1: thionyl chloride / 12 h / Heating

2: 30 percent / Et₃N / CH₂Cl₂ / 1) -20 deg C, 1 h, 2) room temperature 24 h

3: acetonitrile / 8 h / Heating

With thionyl chloride; triethylamine; In dichloromethane; acetonitrile;

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 121612-80-4
5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

Guidance literature:: Multi-step reaction with 6 steps

1: LiAlH₄

3: 55 percent / NaH, 18-crown-6 ether / tetrahydrofuran / 48 h / Ambient temperature

4: 91 percent / hydrazine / ethanol / 3 h / Ambient temperature

5: 30 percent / Et₃N / CH₂Cl₂ / 1) -20 deg C, 1 h, 2) room temperature 24 h

6: acetonitrile / 8 h / Heating

With lithium aluminium tetrahydride; 18-crown-6 ether; sodium hydride; triethylamine; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;

Reference yield:

: 3182-95-4
L-Phenylalaninol

: 121612-80-4
5-((S)-1-Methoxymethyl-2-phenyl-ethylcarbamoyl)-7-methyl-thieno[2,3-b]pyridin-7-ium; iodide

Guidance literature:: Multi-step reaction with 5 steps

2: 55 percent / NaH, 18-crown-6 ether / tetrahydrofuran / 48 h / Ambient temperature

3: 91 percent / hydrazine / ethanol / 3 h / Ambient temperature

4: 30 percent / Et₃N / CH₂Cl₂ / 1) -20 deg C, 1 h, 2) room temperature 24 h

5: acetonitrile / 8 h / Heating

With 18-crown-6 ether; sodium hydride; triethylamine; hydrazine; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;