C₁₇H₁₆N₆O₃

Base Information

Chemical Name:C₁₇H₁₆N₆O₃
CAS No.:1311407-05-2
Molecular Formula:C₁₇H₁₆N₆O₃
Molecular Weight:352.352
Hs Code.:

C<sub>17</sub>H<sub>16</sub>N<sub>6</sub>O<sub>3</sub>

Synonyms:C₁₇H₁₆N₆O₃

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Chemical Property of C₁₇H₁₆N₆O₃

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Technology Process of C₁₇H₁₆N₆O₃

There total 20 articles about C₁₇H₁₆N₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1311407-03-0
C₂₁H₂₂N₆O₄

: 1311407-05-2
C₁₇H₁₆N₆O₃

Guidance literature:: With methanol; ammonia; at 20 ℃; for 60h;
DOI:10.1021/jo2004617

Reference yield:

: 17342-08-4
(S)-Pyroglutaminol

: 1311407-05-2
C₁₇H₁₆N₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1: toluene-4-sulfonic acid / toluene / Reflux

2: lithium hexamethyldisilazane / tetrahydrofuran

3: di-isopropyl azodicarboxylate; acetic acid; triphenylphosphine / tetrahydrofuran

4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

5: pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 24 h / 0 - 20 °C

6: methanol; ammonia / 60 h / 20 °C

With pyridine; methanol; di-isopropyl azodicarboxylate; ammonia; toluene-4-sulfonic acid; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; lithium hexamethyldisilazane; In tetrahydrofuran; toluene; 3: Mitsunobu reaction / 4: Mitsunobu reaction;
DOI:10.1021/jo2004617

Reference yield:

: 100-52-7
benzaldehyde

: 1311407-05-2
C₁₇H₁₆N₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1: toluene-4-sulfonic acid / toluene / 60 h / Reflux; Dean-Stark

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 5 h

3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 24 h / 20 °C

4: pyridine; 1,8-diazabicyclo[5.4.0]undec-7-ene / 24 h / 0 - 20 °C

5: methanol; ammonia / 60 h / 20 °C

With pyridine; methanol; di-isopropyl azodicarboxylate; tetrabutyl ammonium fluoride; ammonia; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; toluene; 3: Mitsunobu reaction;
DOI:10.1021/jo2004617