oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

Base Information

Chemical Name:oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine
CAS No.:85146-06-1
Molecular Formula:C₂₆H₂₇OPS
Molecular Weight:418.54
Hs Code.:

Synonyms:oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

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Chemical Property of oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

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Technology Process of oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

There total 5 articles about oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 85146-03-8
oxyde de (dimethyl-2,3-phenyl-5-pentadienyl-2,4)methylphenylphosphine

: 882-33-7
diphenyldisulfane

: 85146-06-1
oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.5h;

Reference yield:

: 41902-21-0
oxyde de dimethyl-4,5-diphenyl-2,7-oxa-1-phospha-2-cycloheptadiene-4,6

: 85146-06-1
oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

Guidance literature:: Multi-step reaction with 4 steps

1: 72.6 percent / diethyl ether / 2 h / Ambient temperature

2: 93 percent / NaBH₄ / methanol / 2 h / Ambient temperature

3: 68.7 percent / H₂SO₄ / toluene / 2 h / Heating

4: 52 percent / BuLi / tetrahydrofuran / 0.5 h / -78 °C

With sodium tetrahydroborate; n-butyllithium; sulfuric acid; In tetrahydrofuran; methanol; diethyl ether; toluene;

Reference yield:

: 41902-15-2
l'oxyde d'hydroxy-2-dimethyl-4,5-diphenyl-1,2-dihydro-1,2-phosphorine

: 85146-06-1
oxyde de (dimethyl-2,3-phenyl-5-phenylthio-1-pentadienyl-2,4)methylphenylphosphine

Guidance literature:: Multi-step reaction with 5 steps

1: 4 g / Et₃N / toluene / Heating

2: 72.6 percent / diethyl ether / 2 h / Ambient temperature

3: 93 percent / NaBH₄ / methanol / 2 h / Ambient temperature

4: 68.7 percent / H₂SO₄ / toluene / 2 h / Heating

5: 52 percent / BuLi / tetrahydrofuran / 0.5 h / -78 °C

With sodium tetrahydroborate; n-butyllithium; sulfuric acid; triethylamine; In tetrahydrofuran; methanol; diethyl ether; toluene;