N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

Base Information

Chemical Name:N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide
CAS No.:544697-00-9
Molecular Formula:C₃₄H₅₆N₄O₅S₂
Molecular Weight:664.974
Hs Code.:

Synonyms:N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

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Technology Process of N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

There total 2 articles about N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 98-59-9
p-toluenesulfonyl chloride

: 544696-98-2
N-(2-aminoethyl)-3-[(2-aminoethyl)amino]hexadecanamide

: 544697-00-9
N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1002/hlca.200390033

Reference yield:

: methyl hexadec-2-enoate

: 544697-00-9
N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / 24 h / 70 °C

2: 65 percent / Et₃N / CH₂Cl₂ / 12 h / 20 °C

With triethylamine; In dichloromethane; 1: Richman-Atkins procedure;
DOI:10.1002/hlca.200390033

Reference yield: 55.0%

: 4239-24-1
1,6-hexanediol dimethanesulfonate

: 544697-00-9
N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide

: 544696-93-7
1,11-bis[(4-methylphenyl)sulfonyl]-7-tridecyl-1,4,8,11-tetraazacycloheptadecan-5-one

Guidance literature:: N-{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}-3-{{2-{[(4-methylphenyl)sulfonyl]amino}ethyl}amino}hexadecanamide; caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 0.25h;

1,6-hexanediol dimethanesulfonate; In N,N-dimethyl-formamide; at 40 ℃; for 24h;
DOI:10.1002/hlca.200390033