CH₂(P(C₆H₅)2N)2WCl₄

Base Information

Chemical Name:CH₂(P(C₆H₅)2N)2WCl₄
CAS No.:106865-59-2
Molecular Formula:C₂₅H₂₂Cl₄N₂P₂W
Molecular Weight:738.073
Hs Code.:

CH<sub>2</sub>(P(C<sub>6</sub>H<sub>5</sub>)2N)2WCl<sub>4</sub>

Synonyms:CH₂(P(C₆H₅)2N)2WCl₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of CH₂(P(C₆H₅)2N)2WCl₄

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Technology Process of CH₂(P(C₆H₅)2N)2WCl₄

There total 1 articles about CH₂(P(C₆H₅)2N)2WCl₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 53380-82-8
bis[trimethylsilyliminodi(phenyl)phosphoranyl]methane

: 13283-01-7
tungsten(VI) chloride

: 106865-59-2
CH₂(P(C₆H₅)2N)2WCl₄

Guidance literature:: In chloroform; byproducts: Si(CH3)3Cl; dropwise addn. of ligand in dry CHCl3 to a stirred soln. of WCl6 at 0°C; warming up to room temp.; heated (reflux, 24 h);; the ppt. was filtered of and dried (vac.); recrystn. (dry DMF); elem. anal.;;

Reference yield: 66.0%

: 106865-59-2
CH₂(P(C₆H₅)2N)2WCl₄

: CH(P(C₆H₅)2N)2WCl₃

Guidance literature:: With 1,8-diazabicyclo{5.4.0}undec-7-ene; In toluene; byproducts: 1,8-diazabicyclo{5.4.0}undec-7-ene*HCl; dropwise addn. of toluene soln. of DBU to a stirred soln. of WCl4-compd. in toluene; heated (reflux, 10 h);; the ppt. was filtered off, washed (chilled MeCN, 5°C), and dried (vac.); recrystn. (DMF-CH3Cl); elem. anal.;;