(Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester

Base Information

• Chemical Name: (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester
• CAS No.: 74065-01-3
• Molecular Formula: C₃₃H₄₅NO₃
• Molecular Weight: 503.725

Synonyms:(Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester

Chemical Property of (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester

Chemical Property:

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Technology Process of (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester

There total 5 articles about (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl bromide (100-39-0) → (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester (74065-01-3)

Guidance literature:

Multi-step reaction with 4 steps

1: CHCl₃ / Heating

2: 2percent NaOH

3: NaBH₄

With sodium hydroxide; sodium tetrahydroborate; In chloroform;

DOI:10.1021/ja00524a057

Reference yield:

1-((3aS,5aS,6R,9aR)-6-Benzyloxymethyl-dodecahydro-pyrrolo[1,2-a]quinolin-2-yl)-ethanone (74060-05-2,74111-81-2) → (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester (74065-01-3)

Guidance literature:

Multi-step reaction with 4 steps

1: CHCl₃ / Heating

2: 2percent NaOH

3: NaBH₄

With sodium hydroxide; sodium tetrahydroborate; In chloroform;

DOI:10.1021/ja00524a057

Reference yield:

3-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-but-3-en-2-one (74060-07-4) → (Z)-4-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-hex-4-enoic acid ethyl ester (74065-01-3)

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₄

With sodium tetrahydroborate;

DOI:10.1021/ja00524a057

upstream raw materials:

Triethyl orthoacetate

benzyl bromide

3-((2S,4aS,5R,8aR)-1-Benzyl-5-benzyloxymethyl-decahydro-quinolin-2-ylmethyl)-but-3-en-2-one

1-((3aS,5aS,6R,9aR)-6-Benzyloxymethyl-dodecahydro-pyrrolo[1,2-a]quinolin-2-yl)-ethanone

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