Technology Process of 1-(4'-methoxyphenyl)-4,5-methylenedioxybenzocyclobutene
There total 5 articles about 1-(4'-methoxyphenyl)-4,5-methylenedioxybenzocyclobutene which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) sodium hydride / 1.) DMF, 1 h, 2.) DMF, overnight
2: 6 N HCl / benzene / 18 h / Heating
3: 62 percent / n-butyllithium / tetrahydrofuran; diethyl ether / 0.25 h / -95 °C
4: 70 percent / triethylsilane, trifluoroacetic acid / CH2Cl2 / 0.5 h / Ambient temperature
With
hydrogenchloride; triethylsilane; n-butyllithium; sodium hydride; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane; benzene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 62 percent / n-butyllithium / tetrahydrofuran; diethyl ether / 0.25 h / -95 °C
2: 70 percent / triethylsilane, trifluoroacetic acid / CH2Cl2 / 0.5 h / Ambient temperature
With
triethylsilane; n-butyllithium; trifluoroacetic acid;
In
tetrahydrofuran; diethyl ether; dichloromethane;
