6-Methyl-7-oxo-8-phenyl-1λ³-thionia-3λ⁴,5λ⁴-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid

Base Information

• Chemical Name: 6-Methyl-7-oxo-8-phenyl-1λ³-thionia-3λ⁴,5λ⁴-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid
• CAS No.: 75307-82-3
• Molecular Formula: C₈H₈N₅OS₃*Cl
• Molecular Weight: 321.835

Synonyms:6-Methyl-7-oxo-8-phenyl-1λ³-thionia-3λ⁴,5λ⁴-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid

Chemical Property of 6-Methyl-7-oxo-8-phenyl-1λ³-thionia-3λ⁴,5λ⁴-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid

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Technology Process of 6-Methyl-7-oxo-8-phenyl-1λ³-thionia-3λ⁴,5λ⁴-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid

There total 1 articles about 6-Methyl-7-oxo-8-phenyl-1λ³-thionia-3λ⁴,5λ⁴-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

N-Methyl-N'-phenyl-N,N'-bis(trimethylsilyl)harnstoff (1028-22-4) → 6-Methyl-7-oxo-8-phenyl-1λ3-thionia-3λ4,5λ4-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid (75307-82-3)

Guidance literature:

With trithiazyl trichloride; In hexane; for 6h;

Reference yield: 99.0%

antimonypentachloride (7647-18-9) + 6-Methyl-7-oxo-8-phenyl-1λ3-thionia-3λ4,5λ4-dithia-2,4,6,8,9-pentaazabicyclo<3.3.1>nona-2,3,5(9)-trien-chlorid (75307-82-3) → 6-Methyl-7-oxo-8-phenyl-1λ3-thionia-3λ4,5λ4-dithia-2,4,6,8,9-pentaazabicyclo[3.3.1]nona-2,3,5(9)-trien-chlorid (75307-85-6)

Guidance literature:

In tetrachloromethane; ppt. was recrystd. from CH3CN/CCl4 (1:15); elem. anal.;

upstream raw materials:

N-Methyl-N'-phenyl-N,N'-bis(trimethylsilyl)harnstoff

Downstream raw materials:

6-Methyl-7-oxo-8-phenyl-1λ3-thionia-3λ4,5λ4-dithia-2,4,6,8,9-pentaazabicyclo[3.3.1]nona-2,3,5(9)-trien-chlorid

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