ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

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Chemical Name:ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate
CAS No.:1355994-27-2
Molecular Formula:C₁₉H₂₃N₅O₃
Molecular Weight:369.423
Hs Code.:

Synonyms:ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

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Chemical Property of ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

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Technology Process of ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

There total 3 articles about ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 384835-91-0
ethyl 3-amino-1-(4-methoxybenzyl)-1H-pyrazole-4-carboxylate

: 27258-32-8
1-methyl-1H-pyrazole-3-carbaldehyde

: 1355994-27-2
ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

Guidance literature:: ethyl 3-amino-1-(4-methoxybenzyl)-1H-pyrazole-4-carboxylate; 1-methyl-1H-pyrazole-3-carbaldehyde; With sodium tris(acetoxy)borohydride; acetic acid; In dichloromethane; at 0 - 20 ℃; for 24h;

With sodium hydrogencarbonate; In dichloromethane; water;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 1355994-27-2
ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 60 °C

2: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 24 h / 0 - 20 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In dichloromethane; acetonitrile;

Reference yield:

: 6994-25-8,103259-35-4,19750-02-8
3-amino-4-pyrazolecarboxylic acid ethyl ester

: 1355994-27-2
ethyl 1-(4-methoxybenzyl)-3-((1-methyl-1H-pyrazol-3-yl)methylamino)-1H-pyrazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetonitrile / 3 h / 60 °C

2: acetic acid; sodium tris(acetoxy)borohydride / dichloromethane / 24 h / 0 - 20 °C

With sodium tris(acetoxy)borohydride; potassium carbonate; acetic acid; In dichloromethane; acetonitrile;