Technology Process of C27H19NO5
There total 5 articles about C27H19NO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
trifluoroacetic acid;
In
dichloromethane;
at 0 - 20 ℃;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: mineral oil; tetrahydrofuran / 0.5 h / 0 °C
1.2: 12 h / 0 - 20 °C
2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
With
trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1021/ja504624q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: palladium 10% on activated carbon; hydrogen / methanol / 4 h / 20 °C
2.1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / toluene / 20.5 h / 100 °C / Inert atmosphere; Schlenk technique
3.1: mineral oil; tetrahydrofuran / 0.5 h / 0 °C
3.2: 12 h / 0 - 20 °C
4.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
With
palladium 10% on activated carbon; hydrogen; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; toluene; mineral oil;
DOI:10.1021/ja504624q