1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

Base Information

Chemical Name:1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane
CAS No.:110661-81-9
Molecular Formula:C₆₀H₇₈N₆O₁₄S₆
Molecular Weight:1299.71
Hs Code.:

Synonyms:1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

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Chemical Property of 1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

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Technology Process of 1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

There total 3 articles about 1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 35980-64-4
1,5,9-Tritosyl-1,5,9-triazanonane

: 110661-80-8
6,9,12-tris(p-tolylsulfonyl)-6,9,12-triaza-3,15-dioxaheptadecane-1,17-diyl bis(methanesulfonate)

: 110661-81-9
1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 95 ℃; for 72h;
DOI:10.1021/ja00257a024

Reference yield:

: 56187-04-3
1,4,7-tritosyl-1,4,7-triazaheptane

: 110661-81-9
1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

Guidance literature:: Multi-step reaction with 3 steps

2: 98.5 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

3: 44 percent / Cs₂CO₃ / dimethylformamide / 72 h / 95 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00257a024

Reference yield:

: 83076-78-2
6,9,12-triaza-3,15-dioxa-6,9,12-tritosylheptadecane-1,17-diol

: 110661-81-9
1,4,7,13,17,21-hexakis(p-tolylsulfonyl)-1,4,7,13,17,21-hexaaza-10,24-dioxacyclohexacosane

Guidance literature:: Multi-step reaction with 2 steps

1: 98.5 percent / Et₃N / CH₂Cl₂ / 2 h / Ambient temperature

2: 44 percent / Cs₂CO₃ / dimethylformamide / 72 h / 95 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00257a024