2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Base Information

Chemical Name:2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester
CAS No.:241823-97-2
Molecular Formula:C₄₂H₃₀F₇NO₆
Molecular Weight:777.692
Hs Code.:

2-(9<i>H</i>-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Synonyms:2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

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Chemical Property of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

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Technology Process of 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

There total 4 articles about 2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 144120-54-7
Nα-(9-fluorenylmethoxycarbonyl)-L-glutamic acid α-allyl ester

: 241823-94-9
1-[Chloro-bis-(4-fluoro-phenyl)-methyl]-2,3,4,5,6-pentafluoro-benzene

: 241823-97-2
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 14h;

Reference yield:

: 344-04-7
bromopentafluorobenzene

: 241823-97-2
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg / diethyl ether

1.2: 94 percent / diethyl ether / 3 h / Heating

2.1: 100 percent / SOCl₂ / 0.17 h / 20 °C

3.1: 84 percent / DIPEA / CH₂Cl₂ / 14 h / 20 °C

With thionyl chloride; magnesium; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; 1.1: Metallation / 1.2: Grignard reaction / 2.1: Substitution / 3.1: Alkylation;

Reference yield:

: 345-92-6
4,4'-Difluorobenzophenone

: 241823-97-2
2-(9H-fluoren-9-ylmethoxycarbonylamino)-pentanedioic acid 1-allyl ester 5-[bis-(4-fluoro-phenyl)-pentafluorophenyl-methyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg / diethyl ether

1.2: 94 percent / diethyl ether / 3 h / Heating

2.1: 100 percent / SOCl₂ / 0.17 h / 20 °C

3.1: 84 percent / DIPEA / CH₂Cl₂ / 14 h / 20 °C

With thionyl chloride; magnesium; N-ethyl-N,N-diisopropylamine; In diethyl ether; dichloromethane; 1.1: Metallation / 1.2: Grignard reaction / 2.1: Substitution / 3.1: Alkylation;