2-CHLORO-1-(10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-ETHANONE

Base Information

• Chemical Name: 2-CHLORO-1-(10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-ETHANONE
• CAS No.: 3534-05-2
• Molecular Formula: C16H14 Cl N O
• Molecular Weight: 271.74
• Hs Code.: 2933990090
• Mol file: 3534-05-2.mol

Synonyms:5H-Dibenz[b,f]azepine,5-(chloroacetyl)-10,11-dihydro- (7CI,8CI,9CI)

Chemical Property of 2-CHLORO-1-(10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-ETHANONE

Chemical Property:

• Vapor Pressure: 3.51E-09mmHg at 25°C
• Melting Point: 97-100 °C
• Boiling Point: 474.8°Cat760mmHg
• PKA: -2.97±0.20(Predicted)
• Flash Point: 240.9°C
• PSA: 20.31000
• Density: 1.249g/cm³
• LogP: 3.75370

Purity/Quality:

98%Min ^*data from raw suppliers

2-Chloro-1-(10,11-dihydro-dibenzo-[b,f]azepin-5-yl)ethanone ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2-Chloro-1-(10,11-dihydro-dibenzo-[b,f]azepin-5-yl)ethanone (CAS# 3534-05-2) can be used to treat cancer due to its inhibitory effects. It can also be prepared for pharmaceutical use for selective M2 muscarinic receptor antagonists.

Technology Process of 2-CHLORO-1-(10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-ETHANONE

There total 2 articles about 2-CHLORO-1-(10,11-DIHYDRO-DIBENZO[B,F]AZEPIN-5-YL)-ETHANONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

9,10-dihydrodibenzazepine (494-19-9) + chloroacetyl chloride (79-04-9) → 5-chloroacetyl-10,11-dihydro-5H-dibenzazepine (3534-05-2)

Guidance literature:

In toluene; at 90 ℃; for 4h; Inert atmosphere;

DOI:10.1016/j.ejmech.2015.11.023

Reference yield:

→ 5-chloroacetyl-10,11-dihydro-5H-dibenzazepine (3534-05-2)

Guidance literature:

Iminodibenzyl (33), Chloracetylchlorid;

upstream raw materials:

9,10-dihydrodibenzazepine

chloroacetyl chloride

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