C₂₈H₂₄O₆P₂

Base Information

• Chemical Name: C₂₈H₂₄O₆P₂
• CAS No.: 1628202-46-9
• Molecular Formula: C₂₈H₂₄O₆P₂
• Molecular Weight: 518.442
• Mol file: 1628202-46-9.mol

Synonyms:C₂₈H₂₄O₆P₂

Chemical Property of C₂₈H₂₄O₆P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₈H₂₄O₆P₂

There total 5 articles about C₂₈H₂₄O₆P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

C28H24O4P2 (1628202-45-8) → C28H24O6P2 (1628202-46-9)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.666667h; Inert atmosphere; Schlenk technique; Darkness;

DOI:10.1002/chem.201403735

Reference yield:

mesitylphosphine (68357-98-2) → C28H24O6P2 (1628202-46-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: methyllithium / ethylene glycol / 0 °C / Inert atmosphere; Schlenk technique; Reflux

1.2: Inert atmosphere; Schlenk technique; Reflux

2.1: diethyl ether / -78 - 20 °C / Inert atmosphere; Schlenk technique

3.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; tetrahydrofuran / 0.67 h / 20 °C / Inert atmosphere; Schlenk technique; Darkness

With methyllithium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; ethylene glycol;

DOI:10.1002/chem.201403735

Reference yield:

2,4,6-trimethylphenyl bromide (576-83-0) → C28H24O6P2 (1628202-46-9)

Guidance literature:

Multi-step reaction with 4 steps

1.1: magnesium; iodine / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique; Reflux

1.2: 0 - 20 °C / Inert atmosphere; Schlenk technique

1.3: -78 - 20 °C / Inert atmosphere; Schlenk technique

2.1: methyllithium / ethylene glycol / 0 °C / Inert atmosphere; Schlenk technique; Reflux

2.2: Inert atmosphere; Schlenk technique; Reflux

3.1: diethyl ether / -78 - 20 °C / Inert atmosphere; Schlenk technique

4.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane; tetrahydrofuran / 0.67 h / 20 °C / Inert atmosphere; Schlenk technique; Darkness

With methyllithium; iodine; magnesium; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; diethyl ether; dichloromethane; ethylene glycol;

DOI:10.1002/chem.201403735

upstream raw materials:

benzene-1,2,4,5-tetracarbonyl chloride

mesityl[bis(trimethylsilyl)]phosphine

1,2,4,5-benzenetetracarboxylic acid

C₂₈H₂₄O₄P₂