1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane

Base Information

Chemical Name:1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane
CAS No.:68357-99-3
Molecular Formula:C15H29PSi2
Molecular Weight:296.54
Hs Code.:
DSSTox Substance ID:DTXSID10508507
Nikkaji Number:J2.350.481B
Wikidata:Q82365483

Synonyms:68357-99-3;SCHEMBL3293243;DTXSID10508507;1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane

Suppliers and Price of 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 16 raw suppliers

Chemical Property of 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:296.15454099
Heavy Atom Count:18
Complexity:251

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)P([Si](C)(C)C)[Si](C)(C)C)C

Technology Process of 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane

There total 3 articles about 1,1,1,3,3,3-Hexamethyl-2-(2,4,6-trimethylphenyl)disilaphosphane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 75-77-4
chloro-trimethyl-silane

: 68357-98-2
mesitylphosphine

: 68357-99-3
mesityl[bis(trimethylsilyl)]phosphine

Guidance literature:: mesitylphosphine; With methyllithium; In ethylene glycol; at 0 ℃; Inert atmosphere; Schlenk technique; Reflux;

chloro-trimethyl-silane; In ethylene glycol; Inert atmosphere; Schlenk technique; Reflux;
DOI:10.1002/chem.201403735

Reference yield:

: 576-83-0
2,4,6-trimethylphenyl bromide

: 68357-99-3
mesityl[bis(trimethylsilyl)]phosphine

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium; iodine / tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique; Reflux

1.2: 0 - 20 °C / Inert atmosphere; Schlenk technique

1.3: -78 - 20 °C / Inert atmosphere; Schlenk technique

2.1: methyllithium / ethylene glycol / 0 °C / Inert atmosphere; Schlenk technique; Reflux

2.2: Inert atmosphere; Schlenk technique; Reflux

With methyllithium; iodine; magnesium; In tetrahydrofuran; ethylene glycol;
DOI:10.1002/chem.201403735