Technology Process of C25H29NO6
There total 5 articles about C25H29NO6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
4 A molecular sieve; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
at 0 ℃;
for 1.5h;
DOI:10.1002/anie.200605198
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: Bu2BOTf; NEt3 / CH2Cl2 / 0.75 h / 0 °C
1.2: 85 percent / CH2Cl2 / 1 h / 0 °C
2.1: 73 percent / 2,3-dichloro-5,6-dicyan-1,4-benzoquinone; 4 Angstroem molecular sieves / CH2Cl2 / 1.5 h / 0 °C
With
4 A molecular sieve; di-n-butylboryl trifluoromethanesulfonate; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane;
1.2: Evans aldol reaction;
DOI:10.1002/anie.200605198
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 76 percent / diisobutylaluminum hydride / toluene; CH2Cl2 / 0.5 h / -78 °C
2.1: oxalyl chloride; DMSO / CH2Cl2 / 1 h / -45 °C
2.2: 95 percent / NEt3 / CH2Cl2 / 0.25 h / 0 °C
3.1: Bu2BOTf; NEt3 / CH2Cl2 / 0.75 h / 0 °C
3.2: 85 percent / CH2Cl2 / 1 h / 0 °C
4.1: 73 percent / 2,3-dichloro-5,6-dicyan-1,4-benzoquinone; 4 Angstroem molecular sieves / CH2Cl2 / 1.5 h / 0 °C
With
oxalyl dichloride; 4 A molecular sieve; di-n-butylboryl trifluoromethanesulfonate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
dichloromethane; toluene;
3.2: Evans aldol reaction;
DOI:10.1002/anie.200605198
