azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

Base Information

Chemical Name:azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride
CAS No.:1241898-69-0
Molecular Formula:C₁₁H₁₀F₃NO*ClH
Molecular Weight:265.663
Hs Code.:

Synonyms:azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

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Chemical Property of azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

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Technology Process of azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

There total 1 articles about azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1241898-68-9
tert-butyl 3-[2-(trifluoromethyl)benzoyl]azetidine-1-carboxylate

: 1241898-69-0
azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; at 20 ℃; for 3h;

Reference yield:

: 1241897-90-4
ethyl [5-(2-bromo-1,3-thiazol-5-yl)-2H-tetrazol-2-yl]acetate

: 1241898-69-0
azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

: 1241898-70-3
ethyl [5-(2-{3-[2-(trifluoromethyl)benzoyl]azetidin-1-yl}-1,3-thiazol-5-yl)-2H-tetrazol-2-yl]acetate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1-methyl-pyrrolidin-2-one; at 120 ℃; for 0.25h; Sealed tube; Microwave irradiation;

Reference yield:

: 1241897-90-4
ethyl [5-(2-bromo-1,3-thiazol-5-yl)-2H-tetrazol-2-yl]acetate

: 1241898-69-0
azetidin-3-yl[2-(trifluoromethyl)phenyl]methanone hydrochloride

: 1241896-49-0
[5-(2-{3-[2-(trifluoromethyl)benzoyl]azetidin-1-yl}-1,3-thiazol-5-yl)-2H-tetrazol-2-yl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene / ethyl acetate; 1-methyl-pyrrolidin-2-one / 0.25 h / 120 °C / Microwave; Sealed tube

2: water; lithium hydroxide / tetrahydrofuran / 2 h / 20 °C

With water; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; ethyl acetate;