4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE

Base Information

Chemical Name:4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE
CAS No.:328083-79-0
Molecular Formula:C17H24 Cl2 N2 O2
Molecular Weight:359.296
Hs Code.:2933399090
Mol file:328083-79-0.mol

Synonyms:tert-Butyl 1-(3,4-dichlorobenzyl)-4-piperidinylcarbamate

Suppliers and Price of 4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE 95.00%
5MG
$ 498.06

Total 7 raw suppliers

Chemical Property of 4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE

Chemical Property:

Vapor Pressure:2.61E-08mmHg at 25°C
Boiling Point:450.5°C at 760 mmHg
Flash Point:226.3°C
PSA：41.57000
Density:1.23g/cm³
LogP:4.81130

Purity/Quality:

99% ^*data from raw suppliers

4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE

There total 7 articles about 4-TERT-BUTOXYCARBONYLAMINO-1-(3,4-DICHLOROBENZYL)PIPERIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 73874-95-0
(piperidin-4-yl)carbamic acid tert-butyl ester

: 6287-38-3
3,4-dichlorobenzaldehyde

: 328083-79-0
4-tert-butoxycarbonylamino-1-(3,4-dichlorobenzyl)piperidine

Guidance literature:: With sodium tris(acetoxy)borohydride; In chloroform; at 20 ℃; for 20h;
DOI:10.1248/cpb.51.697

Reference yield:

: 73874-95-0
(piperidin-4-yl)carbamic acid tert-butyl ester

: 18880-04-1
3,4-dichlorobenzyl bromide

: 328083-79-0
4-tert-butoxycarbonylamino-1-(3,4-dichlorobenzyl)piperidine

Guidance literature:: With sodium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 3h;

Reference yield:

: 73889-19-7
tert-butyl (1-benzylpiperidin-4-yl)carbamate

: 328083-79-0
4-tert-butoxycarbonylamino-1-(3,4-dichlorobenzyl)piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 24 h

2: tetrahydrofuran / 24 h / Reflux

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol;
DOI:10.1002/ardp.201900371