1,3-bis(2,6-dimethylanilino)propane

Base Information

Chemical Name:1,3-bis(2,6-dimethylanilino)propane
CAS No.:72991-64-1
Molecular Formula:C₁₉H₂₆N₂
Molecular Weight:282.429
Hs Code.:

Synonyms:1,3-bis(2,6-dimethylanilino)propane

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Chemical Property of 1,3-bis(2,6-dimethylanilino)propane

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Technology Process of 1,3-bis(2,6-dimethylanilino)propane

There total 1 articles about 1,3-bis(2,6-dimethylanilino)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72991-64-1
1,3-bis(2,6-dimethylanilino)propane

Guidance literature:: 2,6-Dimethyl-anilin, 1,3-Dibrom-propan, 100grad;

Reference yield: 89.0%

: 72991-64-1
1,3-bis(2,6-dimethylanilino)propane

: 7550-45-0
titanium tetrachloride

: 1106739-96-1
(CH₃)2C₆H₃NH₂(CH₂)3NC₆H₃(CH₃)2TiCl₃⁽¹⁺⁾*Cl^(1-)=(CH₃)2C₆H₃NH₂(CH₂)3NC₆H₃(CH₃)2TiCl₃(Cl)

Guidance literature:: In toluene; (Ar); to soln. of TiCl4 in toluene was added at -20°C soln. of 1,3-(bis(2,6-dimethylanolino)propane in toluene; filtered, washed with pentane, elem. anal.;
DOI:10.1016/j.ica.2008.02.034

Reference yield: 84.0%

: 72991-64-1
1,3-bis(2,6-dimethylanilino)propane

: 7550-45-0
titanium tetrachloride

: 179612-34-1
[Ti(1,3-bis(2,6-dimethylanilino)propane)Cl₂]

Guidance literature:: With (C₂H₅)3N; In toluene; byproducts: (C2H5)3N*HCl; (Ar); soln. of 1,3-(bis(2,6-dimethylanilino)propane in toluene was addedto soln. of TiCl4 ar -78°C, cooling bath was removed, after 15 m in NEt3 was added under vigorous stirring; precipitate was washed with toluene, reduced under vac., cooled to -25°C, crystals was separated, , mother liquor concd., cooled, second batch of crystals was separated;
DOI:10.1016/j.ica.2008.02.034