1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

Base Information

Chemical Name:1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate
CAS No.:59247-63-1
Molecular Formula:C₇H₉N₂O₂*C₉H₁₁O₃S
Molecular Weight:352.411
Hs Code.:

Synonyms:1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

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Chemical Property of 1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

Chemical Property:

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Technology Process of 1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

There total 3 articles about 1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 2459-09-8
4-pyridinecarboxylic acid, methyl ester

: 36016-40-7
mesitylenesulfonylhydroxylamine

: 59247-63-1
1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

Guidance literature:: 4-pyridinecarboxylic acid, methyl ester; mesitylenesulfonylhydroxylamine; In acetonitrile; at 30 ℃; for 0.0166667h; Flow reactor;

With sodium hydroxide; In N,N-dimethyl-formamide; at 30 ℃; for 0.0433333h; Flow reactor;
DOI:10.1055/s-0036-1588799

Reference yield:

: 1239506-69-4
ethyl (1E)-N-(2,4,6-trimethylphenyl)sulfonyloxyethanimidate

: 59247-63-1
1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: perchloric acid / acetonitrile / 0.25 h / 30 °C / Flow reactor

2.1: acetonitrile / 0.02 h / 30 °C / Flow reactor

2.2: 0.04 h / 30 °C / Flow reactor

With perchloric acid; In acetonitrile;
DOI:10.1055/s-0036-1588799

Reference yield:

: 55-22-1
pyridine-4-carboxylic acid

: 59247-63-1
1-amino-4-(methoxycarbonyl)pyridin-1-ium 2,4,6-trimethylbenzene-1-sulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / 72 h / Reflux

2: dichloromethane / 21 h / 0 - 20 °C / Inert atmosphere

With sulfuric acid; In dichloromethane;
DOI:10.1016/j.ejmech.2018.05.043