27-O-acetylmyricerone benzyl ester

Base Information

Chemical Name:27-O-acetylmyricerone benzyl ester
CAS No.:1620542-84-8
Molecular Formula:C₃₉H₅₄O₅
Molecular Weight:602.855
Hs Code.:

Synonyms:27-O-acetylmyricerone benzyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 27-O-acetylmyricerone benzyl ester

Chemical Property:

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Technology Process of 27-O-acetylmyricerone benzyl ester

There total 1 articles about 27-O-acetylmyricerone benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 108-24-7
acetic anhydride

: 100-39-0
benzyl bromide

: 145039-10-7
Myricerone

: 1620542-84-8
27-O-acetylmyricerone benzyl ester

Guidance literature:: acetic anhydride; Myricerone; With pyridine; at 0 ℃; for 3h;

benzyl bromide; With potassium carbonate; In tetrahydrofuran; at 20 ℃; for 16h;
DOI:10.1007/s10600-014-0989-6

Reference yield: 97.0%

: 1620542-84-8
27-O-acetylmyricerone benzyl ester

: 1620542-85-9
12,13-epoxide-27-O-acetylmyricerone benzyl ester

Guidance literature:: With ozone; In ethyl acetate; at -50 ℃;
DOI:10.1007/s10600-014-0989-6

Reference yield:

: 1620542-84-8
27-O-acetylmyricerone benzyl ester

: 3,4-seco-3,4-lactone-12,13-epoxide-27-O-acetylmyricerone benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: ozone / ethyl acetate / -50 °C

2: 3-chloro-benzenecarboperoxoic acid; sodium hydrogencarbonate / dichloromethane

With sodium hydrogencarbonate; ozone; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; ethyl acetate; 2: |Baeyer-Villiger Ketone Oxidation;
DOI:10.1007/s10600-014-0989-6