Technology Process of 6-vinylubiquinone
There total 5 articles about 6-vinylubiquinone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
silver(II) oxide; nitric acid;
In
tetrahydrofuran; water;
at 0 - 20 ℃;
for 0.583333h;
DOI:10.1016/j.tet.2011.06.026
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydroxide / ethanol; water / 0.75 h / Cooling with ice
2.1: titanium tetrachloride / dichloromethane / 4 h / 0 - 20 °C
2.2: 0.17 h / Cooling with ice
3.1: sodium amide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
3.2: 24 h / 20 °C / Inert atmosphere
4.1: silver(II) oxide; nitric acid / tetrahydrofuran; water / 0.58 h / 0 - 20 °C
With
silver(II) oxide; nitric acid; titanium tetrachloride; sodium amide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1016/j.tet.2011.06.026
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: titanium tetrachloride / dichloromethane / 4 h / 0 - 20 °C
1.2: 0.17 h / Cooling with ice
2.1: sodium amide / tetrahydrofuran / 12 h / 20 °C / Inert atmosphere
2.2: 24 h / 20 °C / Inert atmosphere
3.1: silver(II) oxide; nitric acid / tetrahydrofuran; water / 0.58 h / 0 - 20 °C
With
silver(II) oxide; nitric acid; titanium tetrachloride; sodium amide;
In
tetrahydrofuran; dichloromethane; water;
DOI:10.1016/j.tet.2011.06.026