tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Base Information

Chemical Name:tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate
CAS No.:1397495-33-8
Molecular Formula:C₂₀H₂₀O₅
Molecular Weight:340.376
Hs Code.:

Synonyms:tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

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Chemical Property of tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

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Technology Process of tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

There total 3 articles about tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 120-80-9,19481-10-8,37349-32-9
benzene-1,2-diol

: 375349-06-7
tert-butyl 2,3-dihydro-1-oxo-1H-indene-2-carboxylate

: 1397495-33-8
tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: With Pleurotus ostreatus; In aq. phosphate buffer; acetonitrile; at 20 ℃; for 21h; pH=6; Reagent/catalyst; Solvent; pH-value; regioselective reaction; Green chemistry; Enzymatic reaction;
DOI:10.1039/c2gc35662g

Reference yield: 43.0%

: 375349-06-7
tert-butyl 2,3-dihydro-1-oxo-1H-indene-2-carboxylate

: 108-95-2,27073-41-2
phenol

: 1397495-33-8
tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: With activated tyrosinase from Aspergillus oryzae; In acetonitrile; at 20 ℃; for 72h; pH=6; Enzymatic reaction;
DOI:10.1002/ejoc.201800188

Reference yield:

: 5176-27-2
N-tert-butyloxycarbonyl-pyrrole

: 83-33-0
inden-1-one

: 1397495-33-8
tert-butyl 2-(3,4-dihydroxyphenyl)-1-oxo-2,3-dihydro-1H-indene-2-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / mineral oil; tetrahydrofuran / Reflux

2: activated tyrosinase from Aspergillus oryzae / acetonitrile / 72 h / 20 °C / pH 6 / Enzymatic reaction

With activated tyrosinase from Aspergillus oryzae; sodium hydride; In tetrahydrofuran; acetonitrile; mineral oil;
DOI:10.1002/ejoc.201800188