ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate

Base Information

Chemical Name:ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate
CAS No.:83705-11-7
Molecular Formula:C₃₂H₂₇NO₉Se
Molecular Weight:648.528
Hs Code.:

Synonyms:ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate

There total 4 articles about ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 23316-67-8
2,3,5-tri-O-benzoyl-β-D-ribofuranosyl-1-carbonitrile

: 83705-11-7
ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / hydrogen selenide, 4-(dimethylamino)pyridine / 20 h / Ambient temperature

2: 2.5 g / acetonitrile / 1 h / Ambient temperature

With dmap; hydrogen selenide; In acetonitrile;
DOI:10.1021/jm00357a024

Reference yield:

: 6974-32-9
1-O-acetyl-2,3,5-tri-O-benzoyl-β-D-ribofuranose

: 83705-11-7
ethyl 2-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-selenazole-4-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / SnCl₂ / 1,2-dichloro-ethane / 0.03 h

2: H₂Se(g), 4-(dimethylamino)pyridine / ethanol / 0.5 h / 23 °C

3: ethanol / 0.5 h

With dmap; hydrogen selenide; tin(ll) chloride; In ethanol; 1,2-dichloro-ethane;
DOI:10.1002/jhet.5570230132