1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester

Base Information

• Chemical Name: 1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester
• CAS No.: 403664-87-9
• Molecular Formula: C₄₅H₅₆N₂O₂Sn
• Molecular Weight: 776.654

Synonyms:1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester

Chemical Property of 1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester

Chemical Property:

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Technology Process of 1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester

There total 2 articles about 1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)indole-3-carboxylic acid ethyl ester (403664-80-2) → C33H29(2)HN2O2 + C33H28(2)H2N2O2 + 1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester (403664-87-9)

Guidance literature:

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)indole-3-carboxylic acid ethyl ester; With methyllithium; at -65 ℃;

With ethyl [2]alcohol; Further stages.;

DOI:10.1021/ja0120835

Reference yield:

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)indole-3-carboxylic acid ethyl ester (403664-80-2) → C33H28(2)H2N2O2 + 1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester (403664-87-9) + C33H29(2)HN2O2

Guidance literature:

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)indole-3-carboxylic acid ethyl ester; With methyllithium; In tetrahydrofuran; diethyl ether; at -65 ℃;

With ethyl [2]alcohol; In tetrahydrofuran; diethyl ether;

DOI:10.1021/jo030223i

Reference yield: 80.0%

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester (403664-87-9) → (1S,2S)-1,2-(N-tritylaziridino)-2,3-dihydro-1H-pyrrolo[1,2-a]indole-9-carboxylic acid ethyl ester (403664-85-7)

Guidance literature:

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)-2-deutero-indole-3-carboxylic acid ethyl ester; With methyllithium; In tetrahydrofuran; diethyl ether; at -78 - -65 ℃; for 0.416667h;

With Phenylselenyl chloride; In tetrahydrofuran; diethyl ether; at -65 - 20 ℃;

DOI:10.1021/jo030223i

upstream raw materials:

1-(3-tributylstannyl-1-tritylaziridin-2-ylmethyl)indole-3-carboxylic acid ethyl ester

Downstream raw materials:

(1S,2S)-1,2-(N-tritylaziridino)-2,3-dihydro-1H-pyrrolo[1,2-a]indole-9-carboxylic acid ethyl ester

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