Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate

Base Information

Chemical Name:Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate
CAS No.:115929-61-8
Molecular Formula:C₈H₁₀BrNO₄S
Molecular Weight:296.142
Hs Code.:
DSSTox Substance ID:DTXSID301209351

Synonyms:Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate;DTXSID301209351;115929-61-8

Suppliers and Price of Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:294.95139
Heavy Atom Count:15
Complexity:302

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC(=C(C(=C1)Br)OS(=O)(=O)C)N

Technology Process of Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate

There total 3 articles about Phenol, 2-amino-6-bromo-4-methoxy-, 1-methanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 115929-60-7
Methanesulfonic acid 2-bromo-4-methoxy-6-nitro-phenyl ester

: 115929-61-8
3-bromo-2-mesyloxy-5-methoxyaniline

Guidance literature:: With hydrogenchloride; iron; In ethanol; acetic acid; for 2.5h; Heating;
DOI:10.1002/jhet.5570240629

Reference yield:

: 1568-70-3
4-methoxy-2-nitrophenol

: 115929-61-8
3-bromo-2-mesyloxy-5-methoxyaniline

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / Br₂, CH₃COONa / acetic acid / 1) 25 deg C, 30 min; 2) 70 deg C, 2 h

2: 76 percent / pyridine / 24 h / 25 °C

3: 99 percent / Fe, conc. HCl / aq. ethanol; acetic acid / 2.5 h / Heating

With hydrogenchloride; bromine; sodium acetate; iron; In pyridine; ethanol; acetic acid;
DOI:10.1002/jhet.5570240629

Reference yield:

: 115929-59-4
6-bromo-4-methoxy-2-nitrophenol

: 115929-61-8
3-bromo-2-mesyloxy-5-methoxyaniline

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / pyridine / 24 h / 25 °C

2: 99 percent / Fe, conc. HCl / aq. ethanol; acetic acid / 2.5 h / Heating

With hydrogenchloride; iron; In pyridine; ethanol; acetic acid;
DOI:10.1002/jhet.5570240629