(η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)

Base Information

Chemical Name:(η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)
CAS No.:1237501-56-2
Molecular Formula:C₃₄H₅₄N₆NiO₄
Molecular Weight:669.531
Hs Code.:

Synonyms:(η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)

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Chemical Property of (η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)

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Technology Process of (η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)

There total 1 articles about (η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: hexa(μ3-O,O,O'-trimethylacetato)hexa(μ2-O,O'-trimethylacetato)hexanickel(II)

: 3171-45-7
4,5-dimethyl-1,2-phenylenediamine

: 1237501-56-2
(η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)

Guidance literature:: In ethanol; under Ar, Schlenk technique; EtOH added to Ni compd. and diamine, mixt. heated at 60°C until dissolution; filtration, filtrate concd. at 20°C under vac., soln. stored at 20°C for 12 h, crystals sepd. by decantation, washed with cold EtOH and hexane, dried under Ar; elem. anal.;
DOI:10.1007/s11172-009-0002-x

Reference yield: 78.0%

: 64-17-5
ethanol

: 1237501-56-2
(η2-4,5-dimethyl-1,2-phenylenediamino)bis(η1-4,5-dimethyl-1,2-phenylenediamino)bis(η1-pivalato)nickel(II)

: 7732-18-5
water

: tetra(μ3-hydroxo)tris(η1-trimethylacetato)tris(μ2-4,5-dimethyl-1,2-phenylenediamino)tris(η1-4,5-dimethyl-1,2-phenylenediamino)tetranickel(II) trimethylacetate-ethanol-water (1/4/1.5)

Guidance literature:: In ethanol; under Ar, Schlenk technique; EtOH added to Ni compd., mixt. heated 60°C until dissolution; filtration, filtrate concd. at 20°C under vac., soln. stored at 20°C for 12 h, crystals sepd. by decantation, washed with cold ethanol and hexane, dried under Ar; elem. anal.;
DOI:10.1007/s11172-009-0002-x