(1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose

Base Information

Chemical Name:(1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose
CAS No.:1146962-86-8
Molecular Formula:C₄₈H₅₉N₃O₉
Molecular Weight:822.011
Hs Code.:

Synonyms:(1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose

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Technology Process of (1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose

There total 1 articles about (1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₄H₅₅N₃O₇

: 108-24-7
acetic anhydride

: 1146962-86-8
(1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 50 ℃; for 24h; Inert atmosphere;
DOI:10.1002/hlca.200800343

Reference yield: 46.0%

: 74-93-1
methylthiol

: 1146962-86-8
(1R)-1,2-di-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-D-erythro-α-D-galacto-non-2-ulopyranose

: 1146962-91-5
methyl (1R)-1-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-2-thio-D-erythro-α-D-galacto-non-2-ulopyranoside

: 1146962-92-6
methyl (1R)-1-O-acetyl-7-azido-3,4,5,8-tetra-O-benzyl-7,9-dideoxy-1-C-heptyl-2-thio-D-erythro-β-D-galacto-non-2-ulopyranoside

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -30 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1002/hlca.200800343