2-chloro-5-methyl-5-nitro-1,3,2-dioxaphosphinane 2-oxide

Base Information

• Chemical Name: 2-chloro-5-methyl-5-nitro-1,3,2-dioxaphosphinane 2-oxide
• CAS No.: 6533-33-1
• Molecular Formula: C4H7 Cl N O5 P
• Molecular Weight: 215.53

Synonyms:Phosphorochloridicacid, cyclic 2-methyl-2-nitrotrimethylene ester (7CI,8CI); NSC 94245

Chemical Property of 2-chloro-5-methyl-5-nitro-1,3,2-dioxaphosphinane 2-oxide

Chemical Property:

• Vapor Pressure: 0.0447mmHg at 25°C
• Boiling Point: 237.5°Cat760mmHg
• Flash Point: 97.4°C
• Density: 1.54g/cm³

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-chloro-5-methyl-5-nitro-1,3,2-dioxaphosphinane 2-oxide

There total 1 articles about 2-chloro-5-methyl-5-nitro-1,3,2-dioxaphosphinane 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Methyl-2-nitro-1,3-propanediol (77-49-6) → 2-chloro-5-methyl-5-nitro-[1,3,2]dioxaphosphinane 2-oxide (6533-33-1)

Guidance literature:

With trichlorophosphate;

DOI:10.1021/jm00323a034

Reference yield:

2-chloro-5-methyl-5-nitro-[1,3,2]dioxaphosphinane 2-oxide (6533-33-1) + N,N-bis(chloro-2-ethyl)amine (334-22-5) → 2-(Di-(2-chlorethyl)amino)-5-methyl-5-nitro-1,3,2-dioxaphosphorinan-2-oxid (20926-56-1)

Guidance literature:

DOI:10.1002/jps.2600571046

Reference yield:

2-chloro-5-methyl-5-nitro-[1,3,2]dioxaphosphinane 2-oxide (6533-33-1) + 2-phenylethanol (60-12-8) → 2-Phenethyloxy-5-methyl-5-nitro-1,3,2-dioxaphosphorinan-2-oxid (20133-55-5)

Guidance literature:

With triethylamine; In acetone;

DOI:10.1002/jps.2600570937

upstream raw materials:

2-Methyl-2-nitro-1,3-propanediol

Downstream raw materials:

2-(3-Morpholinopropylamino)-5-methyl-5-nitro-1,3,2-dioxaphosphorinane 2-oxide

2-(5'-Fluoranilinium)-5-methyl-5-nitro-1,3,2-dioxaphosphorinan 2-oxid

2-(2'-Fluoranilinium)-5-methyl-5-nitro-1,3,2-dioxaphosphorinan 2-oxid

2-Ethoxy-5-methyl-5-nitro-1,3,2-dioxaphosphorinan-2-oxid

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