2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

Base Information

Chemical Name:2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside
CAS No.:1021450-19-0
Molecular Formula:C₂₉H₃₆N₄O₈Si
Molecular Weight:596.712
Hs Code.:

Synonyms:2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

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Chemical Property of 2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

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Technology Process of 2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

There total 7 articles about 2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₂H₂₅NO₁₁

: 1021450-19-0
2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1: sodium azide / N,N-dimethyl-formamide

2: sodium methylate / methanol

3: toluene-4-sulfonic acid / N,N-dimethyl-formamide

4: dmap; pyridine

5: toluene-4-sulfonic acid / dichloromethane; methanol

6: 1H-imidazole / dichloromethane

With pyridine; 1H-imidazole; dmap; sodium azide; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3sc53471e

Reference yield:

: C₃₀H₂₆N₄O₈

: 1021450-19-0
2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid / dichloromethane; methanol

2: 1H-imidazole / dichloromethane

With 1H-imidazole; toluene-4-sulfonic acid; In methanol; dichloromethane;
DOI:10.1039/c3sc53471e

Reference yield:

: 10022-13-6,31505-44-9,79733-86-1,81704-02-1,116347-84-3,131234-07-6,144300-04-9
1,3,4,6-tetra-O-acetyl-2-phthalimido-2-deoxy-α-D-glucopyranose

: 1021450-19-0
2-azidoethyl 3-O-benzoyl-2-deoxy-2-phthalimido-6-O-tert-butyldimethylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 7 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: sodium azide / N,N-dimethyl-formamide

3: sodium methylate / methanol

4: toluene-4-sulfonic acid / N,N-dimethyl-formamide

5: dmap; pyridine

6: toluene-4-sulfonic acid / dichloromethane; methanol

7: 1H-imidazole / dichloromethane

With pyridine; 1H-imidazole; dmap; sodium azide; boron trifluoride diethyl etherate; sodium methylate; toluene-4-sulfonic acid; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3sc53471e