14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-(diphenyl-methano)-hydrazine

Base Information

• Chemical Name: 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-(diphenyl-methano)-hydrazine
• CAS No.: 1318966-63-0
• Molecular Formula: C₃₅H₃₆N₂O₃
• Molecular Weight: 532.682

Synonyms:14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-(diphenyl-methano)-hydrazine

Chemical Property of 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-(diphenyl-methano)-hydrazine

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Technology Process of 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-(diphenyl-methano)-hydrazine

There total 2 articles about 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-(diphenyl-methano)-hydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

formaldehyd (50-00-0,30525-89-4,61233-19-0) + perfluorobutanesulfonic acid (375-73-5,59933-66-3) + benzophenone hydrazone (5350-57-2) + 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5(10)-trien-3-ol-3-nonafluorbutanesulfonate (1318966-56-1) + C26H25F9O6S (1318966-61-8) + 14,17α-ethanoestra-1,3,5(10)-triene-3,17β-diol (116229-13-1) → 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5(10)-trien-3-ol-3-(diphenyl-methano)-hydrazine (1318966-63-0) + C35H36N2O3 (1318966-66-3)

Guidance literature:

formaldehyd; 14,17α-ethanoestra-1,3,5(10)-triene-3,17β-diol; With triethylamine; magnesium chloride; In tetrahydrofuran; for 8h; Reflux;

perfluorobutanesulfonic acid; With 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 20h;

benzophenone hydrazone; 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-nonafluorbutanesulfonate; C₂₆H₂₅F₉O₆S;

Reference yield:

14,17α-ethanoestra-1,3,5(10)-triene-3,17β-diol (116229-13-1) → 14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5(10)-trien-3-ol-3-(diphenyl-methano)-hydrazine (1318966-63-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: triethylamine; magnesium chloride / tetrahydrofuran / 8 h / Reflux

1.2: 20 h / 0 - 20 °C

2.1: triethylamine; magnesium chloride / tetrahydrofuran / 8 h / Reflux

2.2: 20 h / 0 - 20 °C

With triethylamine; magnesium chloride; In tetrahydrofuran;

upstream raw materials:

formaldehyd

perfluorobutanesulfonic acid

benzophenone hydrazone

14,17-ethano-4-formyl-17-formyloxy-estra-1,3,5⁽¹⁰⁾-trien-3-ol-3-nonafluorbutanesulfonate

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