4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

Base Information

Chemical Name:4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide
CAS No.:1380545-57-2
Molecular Formula:C₁₅H₁₁Cl₂N₃O₃S₂
Molecular Weight:416.309
Hs Code.:

Synonyms:4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

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Technology Process of 4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

There total 2 articles about 4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1380545-52-7
2,4-dichloro-5-(1,3,4-oxadiazol-2-yl)benzenesulfonamide

: 6258-66-8
(4-chlorophenyl)methanethiol

: 1380545-57-2
4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

Guidance literature:: With tetrabutylammomium bromide; potassium carbonate; In water; acetonitrile; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1007/s00706-012-0732-6

Reference yield:

: 18648-15-2
2,4-dichloro-5-(carbazoyl)benzenesulfonamide

: 1380545-57-2
4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / Reflux

2: tetrabutylammomium bromide; potassium carbonate / water; acetonitrile / 24 h / 20 °C / Inert atmosphere

With tetrabutylammomium bromide; potassium carbonate; In water; acetic acid; acetonitrile;
DOI:10.1007/s00706-012-0732-6

Reference yield: 47.0%

: 527-72-0
2-thiophenylcarboxylic acid

: 1380545-57-2
4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide

: 1380545-65-2
4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-N-(thien-2-ylcarbonyl)benzenesulfonamide

Guidance literature:: 2-thiophenylcarboxylic acid; 4-chloro-2-(4-chlorobenzylthio)-5-(1,3,4-oxadiazol-2-yl)-benzenesulfonamide; With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In acetonitrile; at 20 ℃; for 18h;

With toluene-4-sulfonic acid; In acetonitrile;
DOI:10.1007/s00706-012-0732-6