ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate

Base Information

Chemical Name:ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate
CAS No.:1403990-51-1
Molecular Formula:C₂₂H₁₈N₄O₃
Molecular Weight:386.41
Hs Code.:

Synonyms:ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate

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Chemical Property of ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate

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Technology Process of ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate

There total 2 articles about ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1316792-97-8
6-amino-1,3-diphenylbenzo[e][1,2,4]triazin-7-(1H)-one

: 541-41-3
chloroformic acid ethyl ester

: 1403990-51-1
ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate

Guidance literature:: 6-amino-1,3-diphenylbenzo[e][1,2,4]triazin-7-(1H)-one; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 0.25h;

chloroformic acid ethyl ester; In N,N-dimethyl-formamide; mineral oil; at 20 ℃; for 12h;
DOI:10.1021/ol302714j

Reference yield:

: 22751-79-7
1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one

: 1403990-51-1
ethyl (7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-benzylhydoxylamine hydrochloride; N-ethyl-N,N-diisopropylamine / ethanol / 1 h / 20 - 78 °C

2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.25 h / 20 °C

2.2: 12 h / 20 °C

With O-benzylhydoxylamine hydrochloride; sodium hydride; N-ethyl-N,N-diisopropylamine; In ethanol; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol302714j