N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle

Base Information

Chemical Name:N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle
CAS No.:126526-17-8
Molecular Formula:C₂₀H₂₇F₃N₂O₂
Molecular Weight:384.442
Hs Code.:

Synonyms:N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle

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Technology Process of N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle

There total 2 articles about N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 118642-86-7
3-(Dimethyl-hydrazono)-4,4,4-trifluoro-butyric acid ethyl ester

: 126526-15-6
6-iodo-2-phenyl-1-hexene

: 126526-17-8
N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; 1.) 2 h; 2.) 2 h; 3.) 22 h, RT;
DOI:10.1016/S0022-1139(00)82804-3

Reference yield:

: 372-31-6
ethyl 4,4,4-trifluoroacetoacetate

: 126526-17-8
N,N-dimethyl hydrazono-3 trifluoro-4,4,4 (phenyl-5 hexenyl-5)-2 butanoate d'ethyle

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / ethanol / 20 h / Heating

2: 47 percent / 1M LDA; HMPT / tetrahydrofuran / 1.) 2 h; 2.) 2 h; 3.) 22 h, RT

With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide; In tetrahydrofuran; ethanol;
DOI:10.1016/S0022-1139(00)82804-3