C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

Base Information

Chemical Name:C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆
CAS No.:507480-58-2
Molecular Formula:C₇₃H₁₁₆O₁₃S₂Si₃
Molecular Weight:1350.1
Hs Code.:

C<sub>66</sub>H<sub>110</sub>Si<sub>3</sub>SO<sub>11</sub>SO<sub>2</sub>C<sub>7</sub>H<sub>6</sub>

Synonyms:C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

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Chemical Property of C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

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Technology Process of C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

There total 7 articles about C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 98-59-9
p-toluenesulfonyl chloride

: 507480-57-1
Toluene-4-sulfonic acid (E)-(1S,4R,5R,8S,9R)-4,5-bis-(tert-butyl-dimethyl-silanyloxy)-1-[(1R,7S)-7-(tert-butyl-diphenyl-silanyloxy)-1-methoxymethoxy-undecyl]-8-hydroxy-9-methoxymethoxy-hexadec-10-en-15-ynyl ester

: 507480-58-2
C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

Guidance literature:: With pyridine; at 20 ℃; for 17.5h;
DOI:10.1021/jo026433x

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 507480-58-2
C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / pyridine / 24 h / 20 °C

2: H₂ / Pd/C / ethanol / 15.5 h

3: 720 mg / oxalyl chloride; Et₃N; DMSO / CH₂Cl₂ / 1 h / 20 °C

4: 92 percent / InBr₃ / ethyl acetate / 17 h / 20 °C

5: 87 percent / pyridine / 17.5 h / 20 °C

With pyridine; oxalyl dichloride; indium(III) bromide; hydrogen; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; 3: Swern oxidation;
DOI:10.1021/jo026433x

Reference yield:

: 204572-66-7
(4R,5R)-8-Benzyloxy-4,5-bis-(tert-butyl-dimethyl-silanyloxy)-octanal

: 507480-58-2
C₆₆H₁₁₀Si₃SO₁₁SO₂C₇H₆

Guidance literature:: Multi-step reaction with 6 steps

1: 80 percent / InBr₃ / ethyl acetate / 17 h / 20 °C

2: 88 percent / pyridine / 24 h / 20 °C

3: H₂ / Pd/C / ethanol / 15.5 h

4: 720 mg / oxalyl chloride; Et₃N; DMSO / CH₂Cl₂ / 1 h / 20 °C

5: 92 percent / InBr₃ / ethyl acetate / 17 h / 20 °C

6: 87 percent / pyridine / 17.5 h / 20 °C

With pyridine; oxalyl dichloride; indium(III) bromide; hydrogen; dimethyl sulfoxide; triethylamine; palladium on activated charcoal; In ethanol; dichloromethane; ethyl acetate; 4: Swern oxidation;
DOI:10.1021/jo026433x