allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

Base Information

Chemical Name:allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid
CAS No.:908601-86-5
Molecular Formula:C₃₁H₃₄O₈
Molecular Weight:534.606
Hs Code.:

Synonyms:allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

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Chemical Property of allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

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Technology Process of allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

There total 6 articles about allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 908601-84-3
allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranoside

: 908601-86-5
allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

Guidance literature:: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; In phosphate buffer; acetonitrile; for 96h; pH=6.7;
DOI:10.1080/07328300600636819

Reference yield:

: (4aR,6S,7R,8R,8aR)-6-Allyloxy-2-(4-methoxy-phenyl)-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol

: 908601-86-5
allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide

2: LiAlH₄; AlCl₃ / CH₂Cl₂; diethyl ether

3: 95 percent / TEMPO; aq. NaClO₂; aq. NaClO / acetonitrile; aq. phosphate buffer / 96 h / pH 6.7

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; lithium aluminium tetrahydride; aluminium trichloride; sodium hydride; In phosphate buffer; diethyl ether; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1080/07328300600636819

Reference yield:

: (4aR,6S,7R,8S,8aS)-6-Allyloxy-7,8-bis-benzyloxy-2-(4-methoxy-phenyl)-hexahydro-pyrano[3,2-d][1,3]dioxine

: 908601-86-5
allyl 2,3-di-O-benzyl-4-O-p-methoxybenzyl-α-D-galactopyranosiduronic acid

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄; AlCl₃ / CH₂Cl₂; diethyl ether

2: 95 percent / TEMPO; aq. NaClO₂; aq. NaClO / acetonitrile; aq. phosphate buffer / 96 h / pH 6.7

With 2,2,6,6-tetramethyl-piperidine-N-oxyl; sodium hypochlorite; sodium chlorite; lithium aluminium tetrahydride; aluminium trichloride; In phosphate buffer; diethyl ether; dichloromethane; acetonitrile;
DOI:10.1080/07328300600636819