Benzyl 3-isocyanopropionate

Base Information

Chemical Name:Benzyl 3-isocyanopropionate
CAS No.:289707-86-4
Molecular Formula:C₁₁H₁₁NO₂
Molecular Weight:189.214
Hs Code.:

Synonyms:Benzyl 3-isocyanopropionate

Suppliers and Price of Benzyl 3-isocyanopropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl 3-isocyanopropionate

Chemical Property:

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Technology Process of Benzyl 3-isocyanopropionate

There total 3 articles about Benzyl 3-isocyanopropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 34509-32-5
β-Formylaminopropionsaeurebenzylester

: 289707-86-4
Benzyl 3-isocyanopropionate

Guidance literature:: With 4-methyl-morpholine; trichloromethyl chloroformate; In dichloromethane; at -15 ℃;
DOI:10.1039/b002027n

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 289707-86-4
Benzyl 3-isocyanopropionate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / DCC; DMAP

2: 67 percent / diphosgene; N-methylmorpholine / CH₂Cl₂ / -15 °C

With 4-methyl-morpholine; dmap; dicyclohexyl-carbodiimide; trichloromethyl chloroformate; In dichloromethane; 1: Esterification / 2: Dehydration;
DOI:10.1039/b002027n

Reference yield:

: 100-39-0
benzyl bromide

: 289707-86-4
Benzyl 3-isocyanopropionate

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic anhydride / 72 h / 20 °C

1.2: 6 h / 60 °C

2.1: pyridine; p-toluenesulfonyl chloride / dichloromethane / 4.5 h

With pyridine; acetic anhydride; p-toluenesulfonyl chloride; In dichloromethane;