2,3,4-trihydroxyphenyl acetate

Base Information

Chemical Name:2,3,4-trihydroxyphenyl acetate
CAS No.:1618645-23-0
Molecular Formula:C₈H₈O₅
Molecular Weight:184.149
Hs Code.:

Synonyms:2,3,4-trihydroxyphenyl acetate

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Chemical Property of 2,3,4-trihydroxyphenyl acetate

Chemical Property:

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Technology Process of 2,3,4-trihydroxyphenyl acetate

There total 6 articles about 2,3,4-trihydroxyphenyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1618645-01-4
2,3,4-tris(benzyloxy)phenyl acetate

: 1618645-23-0
2,3,4-trihydroxyphenyl acetate

: 1618645-24-1
1,3,4-trihydroxyphenyl acetate

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; methanol; at 25 ℃; under 2325.23 Torr; Overall yield = 100 %; Overall yield = 31 mg;
DOI:10.1039/c4ob00445k

Reference yield:

: 1609113-44-1
benzyl 2,3,4-tris(benzyloxy)benzoate

: 1618645-23-0
2,3,4-trihydroxyphenyl acetate

: 1618645-24-1
1,3,4-trihydroxyphenyl acetate

Guidance literature:: Multi-step reaction with 5 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / Inert atmosphere; Reflux; Sealed tube

2: manganese(IV) oxide / tetrahydrofuran / 8 h / Reflux

3: dihydrogen peroxide; formic acid

4: pyridine / 0 - 20 °C

5: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 25 °C / 2325.23 Torr

With pyridine; manganese(IV) oxide; lithium aluminium tetrahydride; formic acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; In tetrahydrofuran; methanol; 3: |Dakin Phenol Oxidation;
DOI:10.1039/c4ob00445k

Reference yield:

: 1618644-99-7
(2,3,4-tris(benzyloxy)phenyl)methanol

: 1618645-23-0
2,3,4-trihydroxyphenyl acetate

: 1618645-24-1
1,3,4-trihydroxyphenyl acetate

Guidance literature:: Multi-step reaction with 4 steps

1: manganese(IV) oxide / tetrahydrofuran / 8 h / Reflux

2: dihydrogen peroxide; formic acid

3: pyridine / 0 - 20 °C

4: palladium 10% on activated carbon; hydrogen / methanol; tetrahydrofuran / 25 °C / 2325.23 Torr

With pyridine; manganese(IV) oxide; formic acid; palladium 10% on activated carbon; hydrogen; dihydrogen peroxide; In tetrahydrofuran; methanol; 2: |Dakin Phenol Oxidation;
DOI:10.1039/c4ob00445k